HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanecarboxaldehyde → 3-Cyclohexyl-2-dimethoxymethylacrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanecarboxaldehyde | HCID 16275 | — |
| Reactant | 3,3-Dimethoxypropiononitrile | HCID 93731 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Cyclohexyl-2-dimethoxymethylacrylonitrile | HCID 54323403 | — |
Reaction Steps
Cyclohexanecarboxaldehyde (50.0 g, 0.45 mol) was added to a stirred mixture of 3,3-dimethoxypropionitrile (11.5, g, 1.0 mol) and sodium methoxide (54.0 g, 1.0 mol) in methanol over a period of 15 minutes. The mixture was then stirred overnight at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946554B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-0429e80645bb4e15bfebdeef62abd246 |
| Source note | uspto-grants-2005_09 |