HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cuprous chloride → HCID 86593685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cuprous chloride | HCID 62652 | — |
| Reactant | HCID 22323386 | HCID 22323386 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86593685 | HCID 86593685 | — |
Reaction Steps
5 g (13.4 mmole) of 4-isopropoxydinaphtho[2.1-d:1′,2′-f][1,3,2]dioxaphosphepine (rac.-binaphthylisopropyl phosphlte) are dissolved in dichloromethane in a round-bottom flask and 0.44 g (0.45 mmole) of copper(I) chloride is added in a stream of argon. After stirring for 30 minutes the solvent is removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06946577B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-24f7a74a551745f4b3e731bf7b3e56c4 |
| Source note | uspto-grants-2005_09 |