HRID496870

反应详情

EQUATION

反应方程式

HRID 496870 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product from step (iii) was dissolved in dichloromethane (200 ml) and trifluoroacetic acid (100 ml) added. After 18 hrs at room temperature the solvent was evaporated and the resultant gum triturated under ether to give the sub-titled product as a solid (5.7 g).

WORKUP

后处理

  1. customAfter 18 hrs at room temperature the solvent was evaporated
  2. customthe resultant gum triturated under ether