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Triethylamine → tert-Butyl 3-aminopropanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Tert-butyl 3-aminopropanoate hydrochloride | HCID 16218890 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | tert-Butyl 3-aminopropanoate | HCID 4192171 | — |
反応手順
To a solution of β-alanine t-butyl ester hydrochloride (5 mmol, SIGMA) in CH2Cl2 (20 mL) was added triethylamine (5 mmol) at RT After the solution was stirred at RT for 15 mins, the precipitate formed was filtered and the CH2Cl2 was removed in vacuo to give the free amine, β-alanine t-butyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949534B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-0b961f3abcdd4277846e8487a30e5a18 |
| 出典メモ | uspto-grants-2005_09 |