HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 22318113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 73882160 | HCID 73882160 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22318113 | HCID 22318113 | 62% |
Reaction Steps
Gaseous HBr was bubbled into a solution of 18 (3.6 g, 16.1 mmol) in chloroform for 15 minutes. The reaction was diluted with dichloromethane, washed with water, washed with brine, dried (MgSO4), and evaporated in vacuo to afford 3.2 g (62%) of 19 as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949544B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-9fa63202d6a14bb0b52b7bfb68c41335 |
| Source note | uspto-grants-2005_09 |