HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 86589741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 10117829 | HCID 10117829 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86589741 | HCID 86589741 | 90.8% |
Reaction Steps
0.94 g of 1-[2-(4-Methoxyphenyl)-2-(4-methylpiperazino)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine was dissolved in 5.0 ml of ethanol, 5.0 ml of an ethanol solution of 0.56 g of maleic acid was added, followed by being allowed to stand for 2 hours. The precipitated crystals were collected by filtration and washed with ethanol to give 1.24 g of 1-[2-(4-methoxyphenyl)-2-(4-methylpiperazino)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine trimaleate as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949552B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-7c03673d8b334109b822427eb952b587 |
| Source note | uspto-grants-2005_09 |