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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 497329Generated: October 30, 2026

Maleic Acid → HCID 86589742, compound

https://huagongshe.com/reaction/497329

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMaleic AcidHCID 444266—
ReactantHCID 22318639HCID 22318639—
SolventEthanolHCID 702—
ProductHCID 86589742HCID 8658974282.7%

Reaction Steps

0.13 g of 1-[2-(4-Fluorophenyl)-2-(4-isopropylpiperazino)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine was dissolved in 1.5 ml of ethanol, and 1 ml of an ethanol solution of 0.11 g of maleic acid was added, followed by allowing to stand for 2 hours. The precipitated crystals were collected by filtration and washed with ethanol to give 0.18 g of 1-[2-(4-fluorophenyl)-2-(4-isopropylpiperazino)ethyl]-4-(4-naphthalen-1-yl-butyl)piperazine trimaleate as crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06949552B2
Source datasetuspto-grants-2005_09
ORD IDord-88ec01acf1fd4dec901511eb5df64acd
Source noteuspto-grants-2005_09