HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 86589744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 22318636 | HCID 22318636 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86589744 | HCID 86589744 | 62.3% |
Reaction Steps
0.03 g of 1-[2-(4-Fluorophenyl)-2-(4-isopropylpiperazino)ethyl]-4-[4-(2-isopropoxy-naphthalen-1-yl)butyl]piperazine was dissolved in 2.0 ml of ethanol, and 2.0 ml of an ethanol solution of 0.02 g of maleic acid was added, followed by allowing to stand for 2 hours. The precipitated crystals were collected by filtration and washed with ethanol to give 0.03 g of 1-[2-(4-fluorophenyl)-2-(4-isopropylpiperazino)ethyl]-4-[4-(2-isopropoxynaphthalen-1-yl)butyl]piperazine trimaleate as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949552B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-e8c720050ab3455d9d0de4236afee5be |
| Source note | uspto-grants-2005_09 |