HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetic Acid → HCID 22320730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetic Acid | HCID 6227 | — |
| Reactant | Diisopropylcarbodiimide | HCID 12734 | — |
| Reactant | 4-Benzylpiperidine | HCID 31738 | — |
| Product | HCID 22320730 | HCID 22320730 | — |
Reaction Steps
Prepared as stated above for compound (22) from bromo acetic acid (935mg, 6.78 mmol) and 4-benzyl piperdine (1.02 g, 5.82 mmol) and diisopropylcarbodiimide (856 mg, 6.78 mmol) to afford compound 23, 1.53 g, (89%), (MH+) m/z 297.88.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949655B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-251dffb3298f4890b395670388d8d31c |
| Source note | uspto-grants-2005_09 |