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HRID498179

反应详情

EQUATION

反应方程式

HRID 498179 的结构方程式

REACTANTS

反应物

2
结构：CC(C)CN
HCID6558

Isobutylamine

C4H11N

结构：CC(C)(C)OC(=O)Nc1cc(Cl)c(C(F)(F)F)cc1[N+](=O)[O-]
HCID69489376

1,1-Dimethylethyl N-[5-chloro-2-nitro-4-(trifluoromethyl)phenyl]carbamate

C12H12ClF3N2O4

PRODUCTS

生成物

1
结构：CC(C)CNc1cc(NC(=O)OC(C)(C)C)c([N+](=O)[O-])cc1C(F)(F)F
HCID17953218

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

The title compound was prepared from (5-chloro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example A1) (5.00 g, 14.7 mmol), isobutyl-amine (7.36 mL, 73.4 mmol) in DMSO (35 mL) at RT according to the general procedure C. Obtained as a yellow solid (5.39 g, 97%).