HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → 1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 1,1-Dimethylethyl N-(4-chloro-2-nitrophenyl)carbamate | HCID 53980145 | — |
| Product | 1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate | HCID 57456272 | — |
Reaction Steps
The title compound was prepared from (4-chloro-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A5) (22.12 g, 85 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a red solid (13.93 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-dcaeb5058b7a43129313c601914049a9 |
| Source note | uspto-grants-2005_09 |