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HRID498191

反应详情

EQUATION

反应方程式

HRID 498191 的结构方程式

REACTANTS

反应物

2
结构：O.O.[Cl][Sn][Cl]
HCID61436

Stannous chloride dihydrate

Cl2H4O2Sn

结构：CC(C)(C)OC(=O)Nc1ccc(Cl)cc1[N+](=O)[O-]
HCID53980145

1,1-Dimethylethyl N-(4-chloro-2-nitrophenyl)carbamate

C11H13ClN2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1ccc(Cl)cc1N
HCID57456272

1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate

C11H15ClN2O2

PROCEDURE

实验过程

The title compound was prepared from (4-chloro-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A5) (22.12 g, 85 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a red solid (13.93 g).