HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester → tert-butyl N-(2-amino-4-methoxyphenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester | HCID 10730597 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | tert-butyl N-(2-amino-4-methoxyphenyl)carbamate | HCID 10752410 | — |
Reaction Steps
The title compound was prepared from (4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A10) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a white solid (19.377 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-ee5cf85b8e56467cbb1d1bdafadded88 |
| Source note | uspto-grants-2005_09 |