HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (5-methoxy-2-nitrophenyl)carbamate → N1-Boc-5-methoxy-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (5-methoxy-2-nitrophenyl)carbamate | HCID 10199249 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | N1-Boc-5-methoxy-1,2-benzenediamine | HCID 51358605 | — |
Reaction Steps
The title compound was prepared from (5-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A12) (12.234 g, 45.6 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a purple solid (7.185 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-0b03df718d2a4d34bd714fc7d85bf828 |
| Source note | uspto-grants-2005_09 |