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Stannous chloride dihydrate → tert-Butyl (2-amino-4-chloro-5-methylphenyl)carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Stannous chloride dihydrate | HCID 61436 | — |
| 反応物 | HCID 69489578 | HCID 69489578 | — |
| 生成物 | tert-Butyl (2-amino-4-chloro-5-methylphenyl)carbamate | HCID 69486983 | — |
反応手順
The title compound was prepared from (4-chloro-5-methyl-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A17) (4.45 g, 15.5 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a yellow solid (3.90 g, 98%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06949542B2 |
| 出典データセット | uspto-grants-2005_09 |
| ORD ID | ord-ec715028ebe84840b9805c489dc25e6b |
| 出典メモ | uspto-grants-2005_09 |