HCID 69489069, compound → HCID 69489646, compound

HRID 498212Notes

Reaction equation

HRID 498212 reaction equation
[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]1[CH:13]=[C:12]([O:14][CH2:15][CH3:16])[C:11]([Cl:17])=[CH:10][C:9]=1[N+:18]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pt]>[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]1[CH:13]=[C:12]([O:14][CH2:15][CH3:16])[C:11]([Cl:17])=[CH:10][C:9]=1[NH2:18])([CH3:2])([CH3:3])[CH3:4]

Participants

3

Reactant 1

HCID 69489069HCID 69489069, compound

Product 1

HCID 69489646HCID 69489646, compound

Reagents, catalysts & solvents 1

HCID 23939PlatinumCatalyst

Procedure

The title compound was prepared from (4-chloro-5-ethoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example A21) (7.04 g, 22.2 mmol) by hydrogenation with 5% Pt/C according to the general procedure J (method a). Obtained as a light yellow solid (6.32 g, 99%).

Sources & evidence

ORD record
ord-e4ee2800de304081b2c21cb7904fc1bf
Source dataset
uspto-grants-2005_09
Patent number
US06949542B2

Reaction notes

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