HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (5-morpholino-2-nitro-4-(trifluoromethyl)phenyl)carbamate → HCID 12048026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (5-morpholino-2-nitro-4-(trifluoromethyl)phenyl)carbamate | HCID 12048025 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 12048026 | HCID 12048026 | — |
Reaction Steps
The title compound was prepared from (5-morpholin-4-yl-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example C8) (1.83 g, 4.68 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as an amorphous red substance (1.72 g, 102%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-4d58bfc80f50422db21c9243c0945645 |
| Source note | uspto-grants-2005_09 |