HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22317404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86589394 | HCID 86589394 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22317404 | HCID 22317404 | — |
Reaction Steps
The title compound was prepared from {2-[3-oxo-3-(3-pyridin-3-yl-phenyl)-propionylamino]-5-propyl-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (Example M210) (165 mg, 0.31 mmol) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a yellow solid (77 mg, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-1e89bbdeb5b44a25a9ce0d6f0bd1bfe9 |
| Source note | uspto-grants-2005_09 |