HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69486625, compound → HCID 22317736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69486625 | HCID 69486625 | — |
| Reactant | tert-Butyl (2-amino-4-chloro-5-methylphenyl)carbamate | HCID 69486983 | — |
| Product | HCID 22317736 | HCID 22317736 | — |
Reaction Steps
The title compound was prepared from (2-amino-4-chloro-5-methyl-phenyl)-carbamic acid tert-butyl ester (Example J22) (103 mg, 0.4 mmol) and 3-[3-(6-amino-pyrimidin-4-yl)-phenyl]-3-oxo-propionic acid tert-butyl ester (Example K53) (138 mg, 0.44 mmol) according to the general procedure M and subsequent treatment of the crude product according to the general procedure N. Obtained as a light yellow solid (126 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06949542B2 |
| Source dataset | uspto-grants-2005_09 |
| ORD ID | ord-6c5916d5d7ed46df8e7b760710e9f827 |
| Source note | uspto-grants-2005_09 |