HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 68455503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1,3-Cyclohexadiene | HCID 11605 | — |
| Reactant | HCID 68458309 | HCID 68458309 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68455503 | HCID 68455503 | 83.2% |
Reaction Steps
14.5 ml of cyclohexadiene followed by 3.3 g of 10% Pd/C having a 50% water content are added, under an inert atmosphere, to a solution of 6.43 g of the compound obtained in step 6.1, in 50 ml of EtOH. The medium is stirred at AT for 48 hours and then filtered. The filtrate is evaporated, to give 3.63 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767681B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-bcf47c7de33b4504ad255d764bf867f6 |
| Source note | uspto-grants-2010_08 |