HRID49934

反应详情

EQUATION

反应方程式

HRID 49934 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.

WORKUP

后处理

  1. customThe white precipitate thus formed
  2. filtrationwas taken by the filtration
  3. washwashed with water
  4. customdried