HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2913243-44-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl 1-(pyridin-4-yl)piperidine-3-carboxylate | HCID 12895985 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2913243-44-2 | HCID 69142709 | — |
Reaction Steps
A mixture of 1.8 g of ethyl 1-(4-pyridyl)-piperidine-3-carboxylate, 50 ml of dioxane and 20 ml of 1 M hydrochloric acid was heated under reflux for 5 hours. The solvent was evaporated, and the residue was washed with ethyl acetate to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710056B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-8e3b448397e646fe82b0b737be53b5bf |
| Source note | uspto-grants-2004_03 |