HRID49942

反应详情

EQUATION

反应方程式

HRID 49942 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 1.8 g of ethyl 1-(4-pyridyl)-piperidine-3-carboxylate, 50 ml of dioxane and 20 ml of 1 M hydrochloric acid was heated under reflux for 5 hours. The solvent was evaporated, and the residue was washed with ethyl acetate to obtain the title compound.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureunder reflux for 5 hours
  3. customThe solvent was evaporated
  4. washthe residue was washed with ethyl acetate