HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Aminobenzothiazole-6-carboxylic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl 2-Aminobenzothiazole-6-carboxylate | HCID 601008 | — |
| Product | 2-Aminobenzothiazole-6-carboxylic acid hydrochloride | HCID 16236325 | — |
Reaction Steps
500 mg of ethyl 2-aminobenzothiazole-6-carboxylate (Maybridge Co., UK) was stirred in 20 ml of 4 M hydrochloric acid at 80° C. for 5 hours. The solvent was evaporated, and the residue was washed with a solvent mixture of ethyl acetate/hexane to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710056B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-dcb7343d5ea141779291e36914b13022 |
| Source note | uspto-grants-2004_03 |