Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methyl 5-iodo-2-methoxybenzoate | HCID 11011762 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-Iodo-2-methoxybenzoic acid | HCID 4086166 | — |
Reaction Steps
Methyl 2-Methoxy-5-iodobenzoate obtained in step 1 in Example 27 was stirred in a solvent mixture (10 ml) of water and dioxane containing 4 N hydrogen chloride under heating at 80° C. for 3 hours. The solvent was evaporated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06710056B2 |
|---|
| Source dataset | uspto-grants-2004_03 |
|---|
| ORD ID | ord-d4dd423932274b26b287f5bea2bdce86 |
|---|
| Source note | uspto-grants-2004_03 |
|---|
