HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22939443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-(6-Cyano-2-pyridyl)propyl acetate | HCID 22939390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22939443 | HCID 22939443 | 92.3% |
Reaction Steps
3-(6-Cyano-2-pyridyl)propyl acetate (3.0 g, 14.7 mmol) was dissolved in methanol (15 ml), and potassium carbonate (0.08 g, 0.58 mmol) was added thereto. The reaction mixture was stirred at room temperature for 22 hrs and concentrated to give the titled compound (2.2 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767665B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-bb9bf859fb124a6eb520b64cc2685f74 |
| Source note | uspto-grants-2010_08 |