Potassium Carbonate → HCID 22939443, compound

HRID 499573Notes

Reaction equation

HRID 499573 reaction equation
C([O:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([C:14]#[N:15])[N:9]=1)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO>[OH:4][CH2:5][CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]#[N:15])[CH:11]=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 229393903-(6-Cyano-2-pyridyl)propyl acetate

Product 1

HCID 22939443HCID 22939443, compoundYield 92.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

3-(6-Cyano-2-pyridyl)propyl acetate (3.0 g, 14.7 mmol) was dissolved in methanol (15 ml), and potassium carbonate (0.08 g, 0.58 mmol) was added thereto. The reaction mixture was stirred at room temperature for 22 hrs and concentrated to give the titled compound (2.2 g, 92%).

Workup

  1. concentrationconcentrated

Sources & evidence

ORD record
ord-bb9bf859fb124a6eb520b64cc2685f74
Source dataset
uspto-grants-2010_08
Patent number
US07767665B2

Reaction notes

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