HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromo-propoxy)-phenol → HCID 16041752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromo-propoxy)-phenol | HCID 13197597 | — |
| Reactant | 1-Azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol | HCID 42625856 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16041752 | HCID 16041752 | 37% |
Reaction Steps
Following the general procedure outlined in Example 2, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (30.9 mg, 0.111 mmol) and 2-[(3-bromopropyl)oxy]phenol (47.9 mg, 0.207 mmol) in 2 CH3CN/3 CHCl3 (2.5 mL) were reacted to give the desired product (20.9 mg, 37%). EI-MS m/z 430 (M+) Rt (1.70 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-206e802366104acfb024a3b3b52c4311 |
| Source note | uspto-grants-2010_08 |