HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromopropoxy)-3-chlorobenzene → HCID 16041756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromopropoxy)-3-chlorobenzene | HCID 2734929 | — |
| Reactant | 1-Azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol | HCID 42625856 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16041756 | HCID 16041756 | 48% |
Reaction Steps
Following the general procedure outlined in Example 2, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (31.9 mg, 0.114 mmol) and 3-bromopropyl 3-chlorophenyl ether (50.6 mg, 0.203 mmol) in 2 CH3CN/3 CHCl3 (2.5 mL) were reacted to give the desired product (28.7 mg, 48%). EI-MS m/z 448 (M+) Rt (2.0 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-dbe4f1e1620340a6a0edcb9702740519 |
| Source note | uspto-grants-2010_08 |