HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-1-propanol → HCID 16042141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-1-propanol | HCID 12308 | — |
| Reactant | HCID 42625857 | HCID 42625857 | — |
| Product | HCID 16042141 | HCID 16042141 | 31.2% |
Reaction Steps
Following the general procedure outlined in Example 24, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)acetonitrile (0.044 g, 0.152 mmol) and 3-bromo-1-propanol (0.020 mL, 0.282 mmol) in 2CH3CN/3CHCl3 (3.5 mL) were reacted to give the desired product (0.0196 g, 31.1%). EI-MS m/z 333 (M+) Rt (1.43 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-027b9da24cf84cb597d3f25a49b855be |
| Source note | uspto-grants-2010_08 |