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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 499892Generated: October 29, 2026

Hydrochloric Acid → HCID 23116447, compound

https://huagongshe.com/reaction/499892

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 23116190HCID 23116190—
SolventEthanolHCID 702—
ProductHCID 23116447HCID 23116447—

Reaction Conditions

Temperature4 °C

Reaction Steps

Compound 113 (0.6172 g, 1.346 mmol) obtained in Example 112 was dissolved in ethanol (11 mL). The resulting solution was cooled to 4° C., and a 1.0 mol/L solution of hydrogen chloride in ethanol (1.5 mL) was added thereto, followed by stirring for 20 minutes. The reaction mixture was concentrated under reduced pressure to obtain a quantitative yield of Compound 142.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07767693B2
Source datasetuspto-grants-2010_08
ORD IDord-9b870ad6da9d491ab1b38eb97fcff4a0
Source noteuspto-grants-2010_08