Cupric acetate → Cupric acetate

HRID 499934Notes

Reaction equation

HRID 499934 reaction equation
[C:1]([O-:4])(=[O:3])[CH3:2].[Cu+2:5].[C:6]([O-:9])(=[O:8])[CH3:7].O.[NH2:11][NH2:12]>C(O)COCCO>[NH2:11][NH2:12].[C:1]([O-:4])(=[O:3])[CH3:2].[Cu+2:5].[C:6]([O-:9])(=[O:8])[CH3:7]

Participants

5

Reactant 2

HCID 8895Cupric acetateHCID 24654Hydrazine hydrate (1:1)

Product 2

HCID 8895Cupric acetateHCID 9321Hydrazine

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

70 ml of diethylene glycol was added to 8 g of anhydrous copper acetate (manufactured by Wako Pure Chemical Industries, Ltd.). Thereto was added 2.6 ml of 64 wt % hydrazine hydrate at room temperature of 25° C. while stirring so as to give a molar ratio of hydrazine and copper acetate of 1.2, thereby to carry out the reaction. As a result, the resulting precipitate was not cuprous oxide, but copper.

Sources & evidence

ORD record
ord-1638599793c44966a28642ea9bd8a8ad
Source dataset
uspto-grants-2010_08
Patent number
US07767721B2

Reaction notes

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