HCID 178491613, compound → HCID 178491614, compound

Participants

Reaction Steps

The compound (0.3 g) of Example 95 was dissolved in ethanol (15 ml), platinum oxide (50 mg) was added to the solution, and the mixture was hydrogenated at room temperature. After 3 hours, the catalyst was removed by filtration from the reaction mixture and then the solvent was evaporated under reduced pressure. The residue was crystallized from diisopropyl ether to give 0.21 g of the desired compound.

Provenance & Evidence