HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10944665 | HCID 10944665 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1) | HCID 56831841 | — |
Reaction Steps
tert-Butyl (1S)-1-[(dimethylamino)carbonyl]-2-methylpropylcarbamate (131 mg) was treated with 4M of hydrogen chloride in 1,4-dioxane (1.0 mL) at RT for 2 h. The solvent was evaporated under reduced pressure. The residue was dried to give the desired product (96 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767675B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-d0baaf77c7bb4ae8a90fb501b07ccc25 |
| Source note | uspto-grants-2010_08 |