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HRID500177

反应详情

EQUATION

反应方程式

HRID 500177 反应方程式

REACTANTS

反应物

2
Hydrochloric Acid 分子结构式
HCID313

Hydrochloric Acid

ClH

HCID 10944665 分子结构式
HCID10944665

未命名化合物

PRODUCTS

产物

1
N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1) 分子结构式
HCID56831841

N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1)

C7H17ClN2O

AUXILIARIES

试剂、催化剂与溶剂

1
1,4-Dioxane 分子结构式
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

tert-Butyl (1S)-1-[(dimethylamino)carbonyl]-2-methylpropylcarbamate (131 mg) was treated with 4M of hydrogen chloride in 1,4-dioxane (1.0 mL) at RT for 2 h. The solvent was evaporated under reduced pressure. The residue was dried to give the desired product (96 mg).

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure
  2. customThe residue was dried