Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pentacene | HCID 8671 | — |
| Reactant | Maleimide | HCID 10935 | — |
| Solvent | 1,4-Dichlorobenzene | HCID 4685 | — |
| Product | Pentacene maleimide | HCID 86643198 | — |
Reaction Steps
A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07771695B2 |
|---|
| Source dataset | uspto-grants-2010_08 |
|---|
| ORD ID | ord-4208fa9056a44ffda034829caf0cc920 |
|---|
| Source note | uspto-grants-2010_08 |
|---|
