反应详情

温度

160 °C

A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.

1. temperatureThe mixture is cooled to room temperature
2. filtrationthe precipitate is filtered
3. washwashed with toluene
4. customdried
5. customRecrystallization from dichlorobenzene