Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Dipentylamine | HCID 16316 | — |
| Product | 71902-20-0 | HCID 53471076 | — |
Reaction Steps
Diamyl amine (75.13 grams, 0.478 moles) was charged into a 3-neck, round-bottom flask fitted with agitator, condenser, and thermometer. The reactor was placed in cold-water bath, and the CS2 (46.30 grams, 0.608 moles) was added drop-wise through addition funnel while maintaining the reaction temperature under 40° C. The reaction was then placed aspirator vacuum to remove excess CS2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07772170B2 |
|---|
| Source dataset | uspto-grants-2010_08 |
|---|
| ORD ID | ord-ee2c291211e14fd48afb3ec92c2074b4 |
|---|
| Source note | uspto-grants-2010_08 |
|---|
