Carbon Disulfide → 71902-20-0

HRID 500296Notes

Reaction equation

HRID 500296 reaction equation
[CH2:1]([NH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:2][CH2:3][CH2:4][CH3:5].[C:12](=[S:14])=[S:13]>>[CH2:7]([N:6]([CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[C:12](=[S:13])[S-:14])[CH2:8][CH2:9][CH2:10][CH3:11].[CH2:7]([NH2+:6][CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[CH2:8][CH2:9][CH2:10][CH3:11]

Participants

3

Reactant 2

HCID 6348Carbon DisulfideHCID 16316Dipentylamine

Product 1

HCID 5347107671902-20-0

Conditions

Temperature
40 °C

Procedure

Diamyl amine (75.13 grams, 0.478 moles) was charged into a 3-neck, round-bottom flask fitted with agitator, condenser, and thermometer. The reactor was placed in cold-water bath, and the CS2 (46.30 grams, 0.608 moles) was added drop-wise through addition funnel while maintaining the reaction temperature under 40° C. The reaction was then placed aspirator vacuum to remove excess CS2.

Workup

  1. customfitted with agitator, condenser
  2. additionthrough addition funnel
  3. customto remove excess CS2

Sources & evidence

ORD record
ord-ee2c291211e14fd48afb3ec92c2074b4
Source dataset
uspto-grants-2010_08
Patent number
US07772170B2

Reaction notes

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