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HRID500344

反应详情

EQUATION

反应方程式

HRID 500344 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCCCCCCC(=O)O
HCID985

Hexadecanoic acid

C16H32O2

结构：NC1=NC(=O)N([C@H]2C[C@H](O)[C@@H](CO)O2)CN1
HCID178509011

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCC(=O)OC[C@H]1O[C@@H](N2CNC(N)=NC2=O)C[C@@H]1O
HCID178443114

未命名化合物

收率 107.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

2 次

PROCEDURE

实验过程

To a solution of (9) (0.26 g, 1.13 mmol) in MeOH (50 mL) was added a solution of palmitic acid (0.29 g, 1.13 mmol) in hot MeOH (10 mL) and evaporated. The residue was triturated with ether and filtered giving 0.57 g (quantitative yield) of a colorless product with m.p. 123-124°. MS ES+ 231 [M+H+].

WORKUP

后处理

  1. customevaporated
  2. customThe residue was triturated with ether
  3. filtrationfiltered