HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(2,3-Dihydro-1H-inden-2-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Aminoindan hydrochloride | HCID 122764 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-(2,3-Dihydro-1H-inden-2-yl)acetamide | HCID 12452137 | — |
Reaction Steps
Acetic anhydride (3.55 ml) was dropped to the mixture of 6.37 g 2-amino indane hydrochloride, 60 ml of ethyl acetate and 10.4 ml triethylamine and the reaction mixture was stirred at room temperature for 15 hours. The solvents were evaporated in vacuo and the solid residue was digested with water, filtered and dried at 40° C. in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772257B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-c7d4fc384e50469a9368bf8d6b2505af |
| Source note | uspto-grants-2010_08 |