HRID501237

反应详情

EQUATION

反应方程式

HRID 501237 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.6 ml of chloro sulfonic acid was dropped to the stirred solution of 1.06 g N-Indan-2-yl-acetamide and 50 ml of dichloromethane and the mixture was stirred for 15 hours at room temperature. The reaction was than quenched with cold water and die organic phase separated, dried over sodium sulfate evaporated. The resulting residue was used for further reaction without further purification.

WORKUP

后处理

  1. customthan quenched with cold water
  2. customseparated
  3. dry with materialdried over sodium sulfate
  4. customevaporated
  5. customThe resulting residue was used for further reaction without further purification