HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59011488, compound → HCID 59011487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59011488 | HCID 59011488 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 59011487 | HCID 59011487 | 165.8% |
Reaction Steps
400 mg of tert-butyl 5-cyclopropyl-1,1-dioxo-[1,2,5]thiadiazolidine-2-carboxylate were dissolved in 10 ml of CH2Cl2/trifluoroacetic acid 1:1 and left to stand for 2 hours. The volatile constituents were removed in vacuo and coevaporated twice with 50 ml of CH2Cl2 each time. 410 mg of pale yellow oil were obtained and were directly employed further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772262B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-ccd0119f03f94d1c94da0a52a7fff3b5 |
| Source note | uspto-grants-2010_08 |