HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4'-Phenoxyacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Product | 4'-Phenoxyacetophenone | HCID 236783 | — |
Reaction Steps
4-Phenoxyacetophenone was prepared by refluxing 4-fluoroaceotone and phenol in DMAc for 16 hours. The solvent was removed under reduced pressure and the reside subjected to standard ethyl acetate/water work-up and the resulting material purified by silica gel chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772260B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-2336461666234a08953253d8164eb22e |
| Source note | uspto-grants-2010_08 |