HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 501457Generated: October 30, 2026
4-Pyridinecarboxaldehyde → HCID 136059627, compound
https://huagongshe.com/reaction/501457
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 4,5-Diamino-2-methylpyridazin-3(2H)-one | HCID 12727261 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | HCID 136059627 | HCID 136059627 | 42% |
Reaction Steps
0.560 g of 4,5-diamino-2-methyl-2H-pyridazin-3-one and 0.535 g of 4-pyridinecarbaldehyde were added to 10 ml of nitrobenzene, and the mixture was heated at 190° C. under a nitrogen atmosphere for three hours. The reaction solution was cooled down, and the precipitate was collected by filtration to give 0.381 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07772226B2 |
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| Source dataset | uspto-grants-2010_08 |
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| ORD ID | ord-4d8f31411cdd4040a7147e2c401d4e14 |
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| Source note | uspto-grants-2010_08 |
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