HuagongsheHuagongshe Chemistry Print Report · For research reference only
4H,5H,6H,7H-thieno[3,2-c]pyridine-5-carbonyl chloride → 1-(6,7-Dihydro-4H-thieno[3,2-c]pyridine-5-carbonyl)-6-fluoro-1H-indazol-3-yl 6,7-dihydro-4H-thieno[3,2-c]pyridine-5-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4H,5H,6H,7H-thieno[3,2-c]pyridine-5-carbonyl chloride | HCID 79887429 | — |
| Reactant | HCID 178518961 | HCID 178518961 | — |
| Product | 1-(6,7-Dihydro-4H-thieno[3,2-c]pyridine-5-carbonyl)-6-fluoro-1H-indazol-3-yl 6,7-dihydro-4H-thieno[3,2-c]pyridine-5-carboxylate | HCID 68457076 | — |
Reaction Steps
In analogy to example 1, 200 mg (1.315 mmol) of 6-fluoro-1H-indazol-3-ol were reacted with 318 mg (1.578 mmol) of 6,7-dihydro-4H-thieno[3,2-c]pyridine-5-carbonyl chloride. Yield: 18 mg (3%), M+H+: 483.25.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772268B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-fcdf01963ec94b3b89753f2ea04b5fba |
| Source note | uspto-grants-2010_08 |