HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine-4-carbonyl chloride → 6-Fluoro-1-(thiomorpholine-4-carbonyl)-1H-indazol-3-yl thiomorpholine-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine-4-carbonyl chloride | HCID 19080217 | — |
| Reactant | HCID 178518961 | HCID 178518961 | — |
| Product | 6-Fluoro-1-(thiomorpholine-4-carbonyl)-1H-indazol-3-yl thiomorpholine-4-carboxylate | HCID 68459589 | — |
Reaction Steps
In analogy to example 1, 200 mg (1.315 mmol) of 6-fluoro-1H-indazol-3-ol were reacted with 261.4 mg (1.578 mmol) of thiomorpholine-4-carbonyl chloride. Yield: 39 mg (7%), M+H+: 411.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772268B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-e2b12b0309124e0a8e5f15bd285ee800 |
| Source note | uspto-grants-2010_08 |