HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 501489Generated: October 29, 2026
Ethylmorpholine → HCID 72280670, compound
https://huagongshe.com/reaction/501489
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylmorpholine | HCID 7525 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | N-Hydroxy-1,1,1-trimethylsilanamine | HCID 21936899 | — |
| Reactant | HCID 68461196 | HCID 68461196 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72280670 | HCID 72280670 | — |
Reaction Steps
200 mg (0.56 mmol) of 1-(naphthaline-1-sulfonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid were dissolved in 10 ml of DMF, after which 0.61 mmol of ethyl chloroformate, 1.23 mmol of N-ethylmorpholine and 1.68 mmol of trimethylsilylhydroxylamine were added. After the mixture had been heated at 80° C. for 6 h, the solvent was removed under reduced pressure and the crude product was purified using chromatographic methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07772270B2 |
|---|
| Source dataset | uspto-grants-2010_08 |
|---|
| ORD ID | ord-cb3fdb36be514b8293568cd8375ce0aa |
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| Source note | uspto-grants-2010_08 |
|---|
