HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 68461035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 68459735 | HCID 68459735 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68461035 | HCID 68461035 | — |
Reaction Steps
1 g of 1-(4-nitrobenzenesulfonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid (14) was dissolved in 15 ml of DMF, after which 0.1 g of hydrogenation catalyst (10% Pd on active charcoal) was added and the starting compound was quantitatively hydrogenated within 2 h. After the solvent had been removed, the crude product was purified chromatographically.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772270B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-242e08dc46fb43368b8a8ebbe9b17df1 |
| Source note | uspto-grants-2010_08 |