HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18412691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18412339 | HCID 18412339 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18412691 | HCID 18412691 | 96% |
Reaction Steps
Prepared analogously to Example 10 from 2-[N-(4-amidinophenyl)-N-methylaminomethyl]benzothiazol-5-yl-carboxylic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide hydrochloride and sodium hydroxide solution. Yield: 96% of theory, C26H25N5O3S (487.58); Rf value: 0.48 (Merck RP-8, methanol/5% NaCl solution=6:4); EKA mass spectrum: (M+H)+=488; (M+2Na)++=266.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710055B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-aa00afb500994ce2bc2d274293fa27bf |
| Source note | uspto-grants-2004_03 |